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• W1973434818 abstract "(Tl,Pb)(Sr,Ba)2Ca2Cu3Oy single crystals were grown by a self flux method. We find that the crystal growth strictly depends on the starting composition, on optimizing the melting temperature by suitable additives and on the choice of the cooling rate. The crystals were characterized by X-ray diffraction, EDX, SEM and SQUID magnetometry. The supercon-ducting transition temperatures and the best transition widths obtained for as-grown crystals are 105.0–111.2 K and 3–6 K, respectively. Layer by layer growth patterns, but no spiral growth, were observed by SEM. Annealing effects were studied in O2 or Ar atmosphere and led to improvements of Tc and the transition width only following annealing in Ar. Annealing at temperatures above 600°C results in a decomposition of the crystals into the insulating oxides Tl2O and (Sr,Ba)CaCu." @default.
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• W1973434818 date "1996-09-01" @default.
• W1973434818 modified "2023-09-27" @default.
• W1973434818 title "Growth and characterization of (Tl,Pb)(Sr,Ba)2Ca2Cu3Oy single crystals" @default.
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• W1973434818 doi "https://doi.org/10.1016/0022-0248(96)00248-5" @default.
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