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- W1973442783 abstract "The highly stereoselective total synthesis of the phytoalexin (±)-lubiminol (1) has been accomplished. The synthesis relies on three pivotal transformations: (1) a conjugate addition−cyclization reaction to prepare a highly functionalized 2-carbomethoxycyclopentenone as a photocycloaddition substrate, (2) a double diastereoselective intramolecular photocycloaddition for a stereoselective intramolecular photoaddition reaction which establishes the central quaternary spirocenter, and (3) the transformation of the photoadduct into the required spiro[5.4]decane through a radical fragmentation−rearrangement reaction." @default.
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- W1973442783 date "1998-03-01" @default.
- W1973442783 modified "2023-09-25" @default.
- W1973442783 title "Double Diastereoselection in Intramolecular Photocycloadditions: A Radical Rearrangement Approach to the Total Synthesis of the Spirovetivane Phytoalexin (±)-Lubiminol" @default.
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- W1973442783 doi "https://doi.org/10.1021/ja973824y" @default.
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