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- W1973479139 abstract "The thermolysis of nickel acetylacetonate supported on alpha-alumina has been investigated by thermal methods (TGA-DTG-DTA), infrared spectroscopy (FTIR), and X-ray photoelectron spectroscopy (XPS). At 250 degrees C and in static air atmosphere, decomposition of the metal ligands is nearly complete. Higher temperatures are needed in an inert atmosphere or in a vacuum. The variation of XPS peak parameters of samples heated at various temperatures between 120 and 900 degrees C has been interpreted as a change of the distribution of the Ni species between the octahedral and tetrahedral aluminum sites of the support, and a progressive formation of a nickel aluminate-like species, in agreement with temperature-programmed reduction features." @default.
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- W1973479139 date "1999-12-01" @default.
- W1973479139 modified "2023-10-14" @default.
- W1973479139 title "α-Alumina-Supported Nickel Catalysts Prepared with Nickel Acetylacetonate. 2. A Study of the Thermolysis of the Metal Precursor" @default.
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- W1973479139 doi "https://doi.org/10.1021/jp9907286" @default.
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