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- W197349114 abstract "The adducts of M(OAc)2·nH2O (M=Cu, Co, Ni, Zn) with 2-anilinopyridine, M(OAc)2(PhNHpy), have been synthesized and characterized. The X-ray crystal structure of Cu2(μ-OAc)4(PhNHpy)2 shows the dimer structure of Cu2(μ-OAc)4(H2O)2 with the PhNHpy ligand in the axial positions of the water molecules. It is antiferromagnetic (2J=−286 cm−1). Signals of the triplet state are observed in its EPR spectrum and the zero field splitting parameter (D=0.33 cm−1) has been calculated. The electronic spectra and the strong antiferromagnetism of the cobalt (2J=−324 cm−1) and nickel (2J=−382 cm−1) compounds allow to propose also a dimeric structure for them. By excess of ligand, in the anionic form, the Cu(I) compound Cu(PhNpy) was obtained for which a dinuclear structure with a lineal coordination in Cu(I) is proposed." @default.
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- W197349114 date "2002-03-01" @default.
- W197349114 modified "2023-10-07" @default.
- W197349114 title "2-Anilinopyridinate of Cu(I) and adducts of 2-anilinopyridine and metal acetates." @default.
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- W197349114 doi "https://doi.org/10.1016/s0277-5387(01)01015-4" @default.
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