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• W1973708120 abstract "In this work, compounds derived from copper-oxamate anions (ortho, meta, and para)-phenylenebis (oxamate) and imidazolium cations (1-butyl-3-methylimidazolium) were synthesized. The compounds were characterized by Raman and FTIR spectroscopies and the band assignments were supported by DFT calculations. Strong IR bands from 1610 to 1700cm(-1) dominated the spectra of the complex and can be assigned to νCO vibrations of the [Cu(opba)](2-) anions by the comparison with the DFT data. In opposition to the FTIR spectra, the main vibrational bands in the Raman spectra are observed in the 1350-1600cm(-1) range. All bands in this region are associated to the modified benzene vibrations of the copper-phenylenebis(oxamate) anions. X-ray absorption near edge (XANES) at different energies (NK and Cu L2,3 edges) was also used to probe the interionic interactions. XANES data show that anion-cation interaction in the Cu-oxamate-imidazolium changes the electronic structure around the CuN sites in the oxamate anion." @default.
• W1973708120 created "2016-06-24" @default.
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• W1973708120 date "2015-05-01" @default.
• W1973708120 modified "2023-10-10" @default.
• W1973708120 title "Characterization of compounds derived from copper-oxamate and imidazolium by X-ray absorption and vibrational spectroscopies" @default.
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• W1973708120 doi "https://doi.org/10.1016/j.saa.2015.02.012" @default.
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