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• W1973729442 startingPage "741" @default.
• W1973729442 abstract "Lead titanate has been prepared by a sol–gel method using titanium tetrabutoxide and lead acetate in stoichiometric proportion. It was found that the seeding with PbTiO3 nanoparticles (5 and 10 wt.%) into the precursor solution affects the crystallisation process. Thus, unseeded gel calcined at 380°C remained almost amorphous whereas 10 wt.% seeded gel was >70% crystallised. At 400°C, the 10 wt.% seeded sample was almost fully crystallised and the pyrochlore phase was not observed. The isothermal crystallisation kinetics for an unseeded and 5, 10 wt.% seeded PbTiO3 have been compared. The seeded one exhibited enhanced crystallisation kinetics and the activation energy for the PbTiO3 crystallisation was reasonably lowered (from 281 kJ/mol for unseeded to 121 kJ/mol for 10 wt.% seeded gel)." @default.
• W1973729442 created "2016-06-24" @default.
• W1973729442 creator A5016792218 @default.
• W1973729442 creator A5024658416 @default.
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• W1973729442 date "2001-01-01" @default.
• W1973729442 modified "2023-10-17" @default.
• W1973729442 title "Influence of seeding on the crystallisation kinetics of PbTiO3 from gel-derived precursors" @default.
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• W1973729442 doi "https://doi.org/10.1016/s0272-8842(01)00018-9" @default.
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