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• W1973904883 abstract "The optical resolution of (±)-cizolirtine was accomplished with excellent results (>99% ee) by means of crystallization with (+)- or (−)-di-p-toluoyltartaric acid. The optical purity of the samples was controlled by three independent methods: 1H NMR, capillary electrophoresis (CE) (using β-cyclodextrins as chiral resolving agents), and HPLC (using a glycoproteic column). The use of a rapid analytical technique like 1H NMR for estimating the relative amounts of each enantiomer, together with the high sensitivity of CE, afforded a convenient strategy for monitoring the entire process leading to enantiopure compounds. Chirality 11:63–69, 1999. © 1999 Wiley-Liss, Inc." @default.
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• W1973904883 date "1999-01-01" @default.
• W1973904883 modified "2023-10-07" @default.
• W1973904883 title "Optical resolution and enantiomeric purity determination of the analgesic cizolirtine" @default.
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• W1973904883 doi "https://doi.org/10.1002/(sici)1520-636x(1999)11:1<63::aid-chir11>3.0.co;2-k" @default.
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