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- W1974029533 abstract "A synthesis of the antiulcerogenic compound (+)-cassiol 1b has been achieved in 43% yield starting with lactol (S)-2 and sulfone 26. This short and efficient synthesis features the one-pot Julia olefination reaction of the sodium anion of (S)-2 with 26, through the key intermediate (−)-9. This synthesis has been developed as a result of exploratory experiments including different olefination reactions on 2. An attempt to synthesize the intermediate 9 by an intramolecular aldol condensation approach of the open chain precursor 4 is also described." @default.
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- W1974029533 date "2003-03-01" @default.
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- W1974029533 title "Detours en route to a total synthesis of (+)-cassiol" @default.
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- W1974029533 doi "https://doi.org/10.1016/s0957-4166(03)00082-x" @default.
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