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- W1974145608 abstract "Aminomethyl polystyrenes cross-linked with divinylbenzene (PS-DVBs) were prepared by the Lewis acid catalyzed Friedel-Crafts reaction and used as polymer supports in the solid-phase synthesis of polypeptides. The Friedel-Crafts reaction of PS-DVB 1 with N-(chloromethyl)phthalimide 2 in the presence of FeCl3, FeCl3-nitromethane, or FeCl3-benzophenone gave N-(phthaloyl)aminomethyl PS-DVBs 3. The dephthaloylation of PS-DVBs 3 with hydrazine gave aminomethyl PS-DVBs 4a-c. Polypeptide 5 was prepared by using the standard Fmoc procedure with the aminomethyl PS-DVBs 4a-d. The reaction using aminomethyl PS-DVB 4b gave the polypeptide 5 with the highest purity of these polymers." @default.
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- W1974145608 date "2007-02-01" @default.
- W1974145608 modified "2023-09-25" @default.
- W1974145608 title "An Efficient Synthesis of Aminomethyl PS-DVB Using FeCl3-MeNO2 as a Catalyst" @default.
- W1974145608 doi "https://doi.org/10.1055/s-2006-955771" @default.
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