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- W1974152882 startingPage "398" @default.
- W1974152882 abstract "Insertion of tellurium into C–Li bonds of dilithiated 1,2-dicarba-closo-dodecaborane(12) gave 1,2-dicarba-closo-dodecaborano(12)-1,2-ditellurolate [(1,2-C2B10H10)Te2Li2](Et2O) which, after reaction with 1,2-dichlorotetramethyldisilane, afforded a six-membered heterocycle containing the Te–Si–Si–Te unit with an annelated carborane moiety, characterized by multinuclear magnetic resonance and X-ray structural analysis. As a byproduct, a five-membered ring containing a Si–Si–Te unit was formed, which was obtained as a major product, using conditions favouring partial insertion of tellurium into C–Li bonds. Treatment of [(1,2-C2B10H10)Te2Li2](Et2O) with dichlorodimethylsilane led to a five-membered heterocycle as a major product containing a Te–Te–Si unit. Various decomposition/hydrolysis/oxidation products could be identified by multinuclear magnetic resonance, among them most notably 1,2-di(hydrotelluro)-1,2-dicarba-closo-dodecaborane(12)." @default.
- W1974152882 created "2016-06-24" @default.
- W1974152882 creator A5029446593 @default.
- W1974152882 creator A5044451653 @default.
- W1974152882 creator A5079183378 @default.
- W1974152882 date "2012-12-05" @default.
- W1974152882 modified "2023-09-26" @default.
- W1974152882 title "Synthesis of Tellurasila Cycles Containing an Annelated Dicarba‐ <i>closo</i> ‐dodecaborane(12) Unit: Structure of a 1,4‐Ditellura‐2,3‐disilacyclohexane Derivative" @default.
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- W1974152882 doi "https://doi.org/10.1002/ejic.201201124" @default.