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• W1974275359 abstract "The oxidation of oxovanadium(IV) complexes [LV(IV)O] (L = tetradentate Schiff-base ligands such as N,N'-ethylenebis(salicylideneaminate)(2-) (salen) and N,N'-2,2-dimethylpropylenebis(salicylideneaminate)(2-) (salpn)) to [LV(V)O](+), believed to be responsible for the voltammetric response near 0.6 V vs Ag/AgCl in CH(2)Cl(2) in the presence of tetrabutylammonium tetrafluoroborate as a supporting electrolyte, is in fact coupled to a homogeneous process where [LVO](+) coordinates BF(4)(-) to form a neutral complex formulated as [LVOBF(4)]. The formation constants for [VO(salen)BF(4)] and [VO(salpn)BF(4)] are evaluated to be K(salen)(-)(1) = 1.1 x 10(2) M(-)(1) and K(salpn)(-)(1) = 1.4 x 10 M(-)(1), respectively. Crystal structure of [VO(salen)BF(4)] reveals that one of the fluorine atoms in BF(4)(-) is so close to the vanadium(V) atom as to be practically bound in the solid state." @default.
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• W1974275359 date "2003-01-21" @default.
• W1974275359 modified "2023-09-23" @default.
• W1974275359 title "Coordination of BF₄^- to Oxovanadium(V) Complexes, Evidenced by the Redox Potential of Oxovanadium(IV/V) Couples in CH₂Cl₂" @default.
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• W1974275359 doi "https://doi.org/10.1021/ic0205987" @default.
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