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- W1974499439 abstract "Five new lithium aryloxide complexes stabilised by polyamine ligands have been synthesised by simple deprotonation reactions of the parent aryl alcohols H–OAr [OAr = OC6H5, OC6H2-2,4,6-(Me)3 and OC6H2-2,6-(tBu)2-4-(Me)] with LiN(SiMe3)2 in the presence of the Lewis bases N,N,N′,N′-tetramethylethylenediamine (TMEDA) and N,N,N′,N′′,N′′-pentamethyldiethylenetriamine (PMDETA). All the compounds have been characterised by multinuclear NMR and X-ray crystallographic studies. The PMDETA derivative of the phenol adopts a tetrameric ladder-like structural motif in the solid state, exhibiting an unusual bridging coordination mode of the N-donor ligand. The 2,4,6-trimethylphenol derivatives exhibit dimeric (TMEDA), and tetrameric (PMDETA) structural motifs in the solid state. Meanwhile, the TMEDA and PMDETA derivatives of the sterically hindered 2,6-di-tert-butyl-4-methylphenol exhibit a rare monomeric structural motifs, which appears to remain unaltered in C6D6 solution." @default.
- W1974499439 created "2016-06-24" @default.
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- W1974499439 date "2010-01-01" @default.
- W1974499439 modified "2023-10-17" @default.
- W1974499439 title "Structural diversity in polyamine Lewis base stabilised lithium aryloxides" @default.
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- W1974499439 doi "https://doi.org/10.1039/c0dt00522c" @default.
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