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- W1974564462 abstract "Abstract The thermal reaction of Ru 3 (CO) 12 with SC(NMe) 2 in THF at 140°C yields, apart from (μ2-H)Ru 3 (CO) 9 [μ 3 -SRu(CO) 3 (η 2 -CH 2 NMeCNMe 2 )] ( 1 ) ( cf. J. Organomet. Chem., 433 (1992) 149) the carbyne- and dicarbene-containing clusters Ru 4 (CO) 10 (μ 2 -CNMe 2 )-(μ 3 -S)[μ 3 -SRu(CO) 3 (η 2 -CH 2 NMeCNMe 2 )] ( 2 ), Ru 5 (CO) 11 (μ 2 -CNMe 2 ) 2 (μ 4 -S) 2 ( 3 ) and Ru 4 (μ 2 -CO) 3 (CO) 6 (μ 4 -S) 2 (η 2 -Me 2 NCNMeCH 2 CNMe 2 ) ( 4 ). The pentanuclear cluster 3 can also be obtained from the thermolysis of 1 or 2 in THF at 140°C. The structures of the new clusters 2 , 3 and 4 have been solved by single crystal X-ray analyses." @default.
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- W1974564462 date "1992-07-01" @default.
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- W1974564462 title "Rutheniuminduzierter abbau von tetramethylthioharnstoff zu carbin- und dicarbenliganden. Synthese und molekülstruktur der cluster Ru4 (CO)10(μ2-CNMe2)(μ3-S)[μ3-SRu(CO)3(η2-CH2NMeCNMe2)], Ru5(CO)11(μ2-CNMe2)2 (μ4-S)2 und RU4(μ2-CO)3(CO)6(μ4-S)2(η2-Me2NCNMeCH2CNMe2)" @default.
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- W1974564462 doi "https://doi.org/10.1016/0022-328x(92)80139-o" @default.
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