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- W1974673531 abstract "Water-repellent thin films from silane coupling agents have been widely used for inducing hydrophobicity on various surfaces. However, films obtained by conventional methods have poor durability against alkaline solutions. A new water-repellent thin film with high alkali resistance has been obtained for the first time by the sol–gel method using fluoroalkylmethoxysilane and 1,4-bis(trimethoxysilylethyl)benzene (BTB). The film maintained its hydrophobicity after soaking in alkaline ink with pH=8.9 at 70°C for 500 h. While the film maintained alkali resistance after being heat-treated at temperatures up to 300°C, that heat-treated at 400°C lost its alkali resistance. Fourier transform infrared measurements of the film indicated that ethyl groups in BTB molecules burn or oxidize at 400°C. It is speculated that the ethyl groups in the vicinity of siloxane bonds and the three-dimensional BTB polymer network prevent OH-ions from approaching and breaking the siloxane bonds in the film, and thus the film has high alkali resistance. We demonstrate that the new water-repellent film is applicable to the ink jet printer head." @default.
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- W1974673531 date "2002-06-15" @default.
- W1974673531 modified "2023-09-27" @default.
- W1974673531 title "Water-Repellent Thin Film with High Alkali Resistance Using the Sol–Gel Method for Ink Jet Printer Head" @default.
- W1974673531 cites W2124614417 @default.
- W1974673531 doi "https://doi.org/10.1143/jjap.41.3896" @default.
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