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- W1974879244 abstract "Os3(CO)7(1,2-dppm)(μ3-η2:η2:η2-C60) (1) and Os3(CO)7(1,1-dppm)(μ3-η2:η2:η2-C60) (2) were prepared by decarbonylation of Os3(CO)9(μ3-η2:η2:η2-C60) (3) with Me3NO/MeCN in the presence of excess dppm (bis(diphenylphosphino)methane) in chlorobenzene. Then, compounds 1 and 2 were characterized by obtaining spectroscopic and microanalytical data, as well as by performing single-crystal X-ray diffraction studies. In addition, the electrochemical properties of 1 and 2 were examined by performing cyclic voltammetry. The cyclic voltammograms suggest that a C60-mediated electron transfer to the osmium cluster center takes place for species 13− and 23− in compounds 1 and 2." @default.
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- W1974879244 date "2014-08-01" @default.
- W1974879244 modified "2023-10-14" @default.
- W1974879244 title "Synthesis, characterization, and electrochemical study of Os3(CO)7(1,2-dppm)(μ3-η2:η2:η2-C60) and Os3(CO)7(1,1-dppm)(μ3-η2:η2:η2-C60)" @default.
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- W1974879244 doi "https://doi.org/10.1016/j.jorganchem.2014.04.016" @default.
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