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- W1974887675 abstract "Poly(ethylene glycol) (PEG)-silk fibroin (SF) conjugate (PEG1-SF) was prepared by the chemical modification of solubilized SF with 2-[O-methoxypoly(ethylene glycol)]-4,6-dichloro-s-triazine (actPEG1), and the physical properties of the PEG1-SF film were studied. The circular dichroism (c.d.) spectrum of the PEG1-SF film exhibited both negative and positive extrema due to a β-sheet structure. D.s.c. measurements and polarizing microscopic observations at elevating temperature of the PEG1-SF film clarified the thermal behaviour of the PEG1-SF film exhibiting the melting of the PEG chains and the decomposition of SF. In the d.s.c. thermogram of PEG1-SF, the positions of the endothermic peaks due to the melting of the PEG chains and the decomposition of SF scarcely shifted compared to the peak position of actPEG1 and the peak position of the SF having a β-sheet structure, respectively. Judging from these observations, the mutual miscibility between PEG and SF was considered to be poor. The tensile tests of the PEG1-SF and SF films revealed that the PEG-modification of SF improved the elongation at break but reduced the tensile strength. based on these results, a layered structure of the PEG1-SF film was suggested." @default.
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- W1974887675 date "1997-01-01" @default.
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- W1974887675 title "Physical properties and structure of poly(ethylene glycol)-silk fibroin conjugate films" @default.
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- W1974887675 doi "https://doi.org/10.1016/s0032-3861(96)00665-9" @default.
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