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• W1975936237 abstract "The zinc (II) complex with nicotinamide, (C6H11N2)[ZnBr3(C6H6N2O)], was prepared under ionothermal condition by using the ionic liquid 1-ethyl-3-methylimidazolium bromide ([EMIM]Br) as a solvent. At the same time, [EMIM]Br also functions as a structure-directing agent, leading to a framework structure different from those obtained by the conventional methods. Single-crystal X-ray analysis revealed that the coordinated compound crystallizes in monoclinic space group P2(1)/c, and the Zn (II) ion is four-coordinated by one pyridine ring N atom and three bromide anions in a slightly distorted tetrahedron arrangement. The [EMIM]+ cations acting as the extra framework charge balancing species occupy the channels of this asymmetric unit. In the crystal structure, intermolecular NH⋯Br and NH⋯O hydrogen bonds link the molecules to form a supramolecular structure. In addition, this compound was further characterized by FT-IR and Raman spectroscopic techniques, and the observed important bands were assigned. Thermogravimetric analysis (TG), Differential Scanning Calorimetry (DSC) and fluorescent properties of solid samples were also studied at room temperature." @default.
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• W1975936237 date "2015-01-01" @default.
• W1975936237 modified "2023-10-16" @default.
• W1975936237 title "Ionothermal synthesis, properties and vibrational spectra of zinc (II) complex with nicotinamide" @default.
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• W1975936237 doi "https://doi.org/10.1016/j.saa.2014.06.080" @default.
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