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- W1975952112 abstract "A multistep synthetic route to (±)-10-[2-(1-methyl-2-piperidinyl)ethyl]-2-methylthio-10H-phenothiazine (thioridazine) was developed which allowed for the incorporation of two deuterium atoms in the piperidine ring and a further two in the 1-position of the ethyl side chain. The key steps involved ruthenium tetroxide oxidation of N-protected methyl 2-piperidinylacetate and subsequent lithium aluminum deuteride reduction of 2-(2-hydroxyethyl)-1-methyl-6-piperidinone or the corresponding piperidinoneester. The isotopic purity of the dideuterated and tetradeuterated products was greater than 99%." @default.
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- W1975952112 date "1988-04-01" @default.
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- W1975952112 title "Synthesis of deuterium labelled thioridazine via ruthenium tetroxide oxidation of the piperidine ring" @default.
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- W1975952112 doi "https://doi.org/10.1002/jlcr.2580250408" @default.
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