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- W1976179962 abstract "Abstract Three unknown olivacine derivatives ( L ‐OCH 3 , L ‐OH, L ‐OAc) were synthesized according to a procedure that involves only a few steps, and used as ligands in the synthesis of neutral chelate platinum( II ) complexes. The ligands, as well as their platinum complexes were spectroscopically characterized with IR, 1 H/ 13 C NMR and UV/Vis spectroscopic techniques. The solid state structures of two ligands ( L ‐OCH 3 , L ‐OAc) and one complex {[( L ‐OCH 3 )PtCl 2 ]} were determined by X‐ray diffraction. Molecular structure analysis of the ligands and the complex indicated that complexation resulted in a change in the conformation of the bipyridine fragment of the compounds studied and caused other interesting effects. Two crystallographically independent molecules of the complex were revealed in the measured crystal, with short intramolecular H ··· H distances. The structural and energetic aspects of the conformational behavior of the ligand L ‐OCH 3 and the complex [( L ‐OCH 3 )PtCl 2 ] have been analyzed using semiempirical PM3 methods. In vitro antiproliferative activity was preliminarily estimated. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)" @default.
- W1976179962 created "2016-06-24" @default.
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- W1976179962 date "2003-11-01" @default.
- W1976179962 modified "2023-10-17" @default.
- W1976179962 title "Synthesis, Structure and Characterization of New Olivacine Derivatives and Their Platinum(<scp>II</scp>) Complexes" @default.
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- W1976179962 doi "https://doi.org/10.1002/ejic.200300291" @default.
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