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• W1976290465 abstract "Nanocrystalline aluminum oxide films have been synthesized by r.f. reactivesputtering deposition, and their structure and properties have been studied by grazing angle X-ray diffraction, nanoindentation and transmission electron microscopy. The as-deposited films contained nanocrystalline γ−Al2O3 embedded in an amorphous Al2O3 matrix. Annealing of the films between 800 and 1200°C resulted in crystallization of the amorphousAl2O3 matrix. various degrees of γ→α phase transformation. Prolonged anneals of the films at 800 °C for 24h gave arise to the development of structural texture in γ−Al2O3 grains. No appreciable grain growth of γ−Al2O3 was detected in the films annealed at temperatures below 1200°C. Annealing of the films at 1200°C for 2 h resulted in the formation of explosively grown, single-crytsal α−Al2O2 grains in a highly textured, polycrystalline γ−Al2O3 matrix. The microstructure of γ−Al2 O3 exhibited an intriguing layered characteristic. These layers were aligned consistently throughout the films; most of them were oriented at 90° to each other. The layered microstructure is believed to be the characteristic of an intermediate state during γ→α transformation, which contributes to the concurrent explosive grain growth of α−Al2O3. The nucleation of γ-Al2O3 is suggested to occur along the {220} crystallographic planes of γ−Al2O3.Preliminary micromechanical properties of as-deposited nanocrystalline Al2O3 films are reported." @default.
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• W1976290465 date "1991-12-01" @default.
• W1976290465 modified "2023-09-23" @default.
• W1976290465 title "Microstructural evolution and properties of nanocrystalline alumina made by reactive sputtering deposition" @default.
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• W1976290465 doi "https://doi.org/10.1016/0040-6090(91)90294-8" @default.
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