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• W1976362976 abstract "Dioxomolybdenum(VI) complexes of the type MoO2X2L containing ethylenediimine ligands were prepared in good yield by reaction of MoO2X2(THF)2 (X = Cl, Br) with the bidentate ligands Ph2CNCH2CH2NCPh2 (PBED) or PhCHNCH2CH2NCHPh (BED). The crystal structure of MoO2Br2(BED) was determined by X-ray diffraction. The dichloro complexes were active as catalysts for the reaction of cyclooctene with tert-butyl hydroperoxide (TBHP) at 55 °C yielding epoxycyclooctane as the only product up to 7 h after the start of the reaction. The highest initial activity was obtained with MoO2Cl2(BED) (63 mol molMo−1 h−1). Other olefins were also tested, and activities decreased in the order cyclooctene > cyclododecene > (R)-(+)-limonene > cyclohexene > trans-2-octene > 1-octene. The dibromo complexes exhibited much lower activities than the dichloro complexes for the epoxidation of cyclooctene." @default.
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• W1976362976 date "2005-03-01" @default.
• W1976362976 modified "2023-09-23" @default.
• W1976362976 title "Preparation and catalytic studies of bis(halogeno)dioxomolybdenum(VI)-diimine complexes" @default.
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• W1976362976 doi "https://doi.org/10.1016/j.molcata.2004.10.004" @default.
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