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- W1976593404 abstract "Abstract Treatment of the tungsten compounds [W(CR)Br(CO) 4 ] (R = C 6 H 4 Me-4, C 6 H 4 OMe-2, or C 6 H 3 Me 2 -2,6) in tetrahydrofuran with the salts K[HB(3,5-Me 2 pz) 3 ][HB(3,5- Me 2 pz) 3 = hydrotris(3,5-dimethylpyrazol-1-yl)borate], K[HB(3-Phpz) 3 ] [HB(3-Phpz) 3 = hydrotris(3-phenylpyrazol-1-yl)borate] and K[HB(pz) 3 ] [HB(pz) 3 = hydrotris(pyrazol-1-yl) borate], affords, respectively, the complexes [W(CC 6 H 4 Me-4)(CO) 2 {HB(3,5-Me 2 pz) 3 }], [W(C 6 H 4 Me-4)(CO) 2 {HB(3-Phpz) 3 }] and [W(CR)(CO) 2 {HB(pz)3}] (R = C 6 H 3 Me 2 -2,6 or C 6 H 4 OMe-2). Protonation of the compound [W(CC 6 H 4 OMe-2)(CO) 2 {HB(pz) 3 }] with HBF 4 ·Et 2 O gives the salt [W{C(H) C 6 H 4 OMe-2}(CO) 2 {HB(pz) 3 }][BF 4 ]. The NMR data for the new complexes are reported and discussed." @default.
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- W1976593404 date "1991-01-01" @default.
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- W1976593404 title "Synthesis of alkylidyne tungsten complexes with hydrotris(pyrazol-1-yl)borate ligands" @default.
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- W1976593404 doi "https://doi.org/10.1016/s0277-5387(00)81591-0" @default.
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