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- W1976662940 abstract "[1,4]-Diazepan-6-ols are easily oxidized to ketones using Swern or Dess-Martin oxidation conditions. The fluorination of these [1,4]-diazepanones with diethylaminosulfur trifluoride (DAST) affords gem-difluorohomopiperazines. Detosylation under microwave conditions represents a rapid method to access the corresponding amines in high yields." @default.
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- W1976662940 date "2003-01-01" @default.
- W1976662940 modified "2023-09-26" @default.
- W1976662940 title "Synthesis of 6,6-Difluorohomopiperazines via Microwave-Assisted Detosylation" @default.
- W1976662940 doi "https://doi.org/10.1055/s-2003-36834" @default.
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