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• W1976850646 abstract "The direct selective separation of the trivalent actinides americium and curium from a simulated Plutonium Uranium Refining by EXtraction (PUREX) raffinate solution by a continuous counter-current solvent extraction process using miniature annular centrifugal contactors was demonstrated on a laboratory scale. In a 32-stage spiked test (12 stages for extraction, 16 stages for scrubbing, and 4 stages for Am/Cm stripping), an extractant mixture of CyMe4BTBP and TODGA in a TPH/1-octanol mixture was used. The co-extraction of some fission and corrosion product elements, such as zirconium and molybdenum, was prevented by using oxalic acid. Co-extracted palladium was selectively stripped using an L-cysteine scrubbing solution and the trivalent actinides were selectively stripped using a glycolic acid-based stripping solution. It was demonstrated that a selective extraction and high recovery of > 99.4% of the trivalent minor actinides was achieved with low contamination by fission and corrosion products. The product contained 99.8% of the initial americium and 99.4% of the initial curium content. The spent solvent still contained high concentrations of Cu, Cd, and Ni. The experimental steady-state concentration profiles of important solutes were determined and compared with those from computer-code calculations." @default.
• W1976850646 created "2016-06-24" @default.
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• W1976850646 date "2013-03-01" @default.
• W1976850646 modified "2023-09-26" @default.
• W1976850646 title "Direct Selective Extraction of Actinides (III) from PUREX Raffinate using a Mixture of CyMe₄BTBP and TODGA as 1-cycle SANEX Solvent Part III: Demonstration of a Laboratory-Scale Counter-Current Centrifugal Contactor Process" @default.
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• W1976850646 doi "https://doi.org/10.1080/07366299.2013.775890" @default.
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