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• W1976940711 abstract "The present work reports the solvent-free, one-pot functionalization of multiwall carbon nanotubes (CNTs) based on the 1,3-dipolar cycloaddition of azomethine ylides using N-benzyloxycarbonyl glycine and formaldehyde. The surface morphology of the functionalized CNTs was investigated by scanning tunneling microscopy. The effect of temperature on the reaction was studied by thermogravimetry and X-ray photoelectron spectroscopy (XPS). XPS was a key technique for the detailed chemical analysis of the CNT surface. The formation of two major reaction products was observed, namely a cyclic benzyl carbamate and a pyrrolidine. The concentration of the two products varied with reaction temperature and time. At 180 °C, the main product was the cyclic benzyl carbamate, while at 250 °C the major product was the pyrrolidine. This simple, solvent-free chemical procedure yields CNTs with fine-tuned surface functionality." @default.
• W1976940711 created "2016-06-24" @default.
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• W1976940711 date "2010-11-30" @default.
• W1976940711 modified "2023-10-17" @default.
• W1976940711 title "Controlled Functionalization of Carbon Nanotubes by a Solvent-free Multicomponent Approach" @default.
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• W1976940711 doi "https://doi.org/10.1021/nn1022523" @default.
• W1976940711 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/21117643" @default.
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