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- W1977305894 abstract "Atom transfer radical polymerization (ATRP) was used to prepare poly(acetoxystyrene) (PAS) with a controlled molecular weight and narrow polydispersity. Using 1-phenylethylbromide (PEBr)/CuBr/Cu(0)/2,2′-bipyridine as an initiating system, the heterogeneous ATRP of 4-acetoxystyrene was carried out to form PAS as a precursor polymer. The reaction follows the first-order kinetics with respect to the conversion of monomer. A linear molecular weight (polydispersities Mw/Mn = 1.07–1.27) indicates the “living”/controlled nature of polymerization. The obtained PAS was chemically modified to obtain succinylated poly(hydroxystyrene) (Succ-PHS). The formulation of Succ-PHS, crosslinker (benzoguanamine-formaldehyde), and triphenylsulfonium triflate (TPST) as a photo acid generator (PAG) was carried out by UV irradiation using an i-line tool. The performance of the resultant polymer as the negative resist pattern photoresist for photolithography was studied with instrumental techniques. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 3560–3566, 2007" @default.
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- W1977305894 date "2006-01-01" @default.
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- W1977305894 title "Synthesis of succinylated poly(4-hydroxystyrene) and its application for negative-tone photoresist" @default.
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- W1977305894 doi "https://doi.org/10.1002/app.24979" @default.
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