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• W1977338267 abstract "Condensation of aminoguanidine with 2-formylpyridine, 2-benzoylpyridine and 2,6-diacetylpyridine results in the aminoguanidones, HFogu, HBzgu and H 2 2,6Acgu 2 , respectively. Reaction of the heterocyclic aminoguanidone in a mixture of hydrochloric acid–ethanol with copper(II) chloride produces the following mixed salts: [H 3 Fogu][CuCl 4 ], ( 1 ), [H 3 Bzgu] 2 [CuCl 4 ]Cl 2 ·H 2 O, ( 2 ), and [H 5 2,6Acgu 2 ][CuCl 4 ]Cl·H 2 O, ( 3 ). Their crystal structures, as well as their ESR and UV spectra, have been obtained. The influence on the geometry of the [CuCl 4 ] 2− of the NH⋯ClCu hydrogen bonds, in the context of charged compensation hypothesis, has been evaluated. The synthesis, crystal structure, ESR and UV spectra of three copper(II) halide anions with aminoguanidonium cations derived from 2-formylpyridine, 2-benzoylpyridine and 2,6-diacetylpyridine is reported. [CuCl 4 ] 2− derivatives were obtained. Extended hydrogen bonding networks are present in all of them. The charge compensation approach fails to predict the geometry of the [CuCl 4 ] 2− ions." @default.
• W1977338267 created "2016-06-24" @default.
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• W1977338267 date "2002-03-01" @default.
• W1977338267 modified "2023-10-18" @default.
• W1977338267 title "Tetrachlorocuprate(II) salts of heterocyclic aminoguanidonium (guanylhydrazonium) ions" @default.
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• W1977338267 doi "https://doi.org/10.1016/s0277-5387(01)01006-3" @default.
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