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- W1977573766 abstract "Abstract The reactions of [(H5C6)3P]2ReH6− with (CH3CN)3Cr(CO)3, (diglyme)Mo(CO)3 or (C3H7CN)3W(CO)3 led to the formation of [(H5C6)3P]2ReH6M(CO)3− (M = Cr, Mo, W) complexes. These have been characterized by IR and NMR spectroscopies, as well as elemental analyses. A single crystal X-ray diffraction study has also been carried out for the M = Cr complex as a K(18-crown-6)+ salt. The complex crystallizes as a THF monosolvate in the monoclinic space group P21/n with a = 22.323(6), b = 9.523(2), c = 27.502(5) A , β = 104.98(2) 0 and V = 5648 A 3 for Z = 4 . The ReCr separation is 2.5745(12) A, and the two phosphine ligands are oriented unsymmetrically. Although the hydride ligands were not found, the presence of three bridging hydrides and a dodecahedral coordination geometry about rhenium could be inferred. Low temperature 1H and 31P NMR spectroscopic studies did not reveal the low symmetry of the solid state structure." @default.
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- W1977573766 date "1995-12-01" @default.
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- W1977573766 title "The ReH6[P(C6H5)3]2− ion as a ligand: complexes with M(CO)3 fragments (M = Cr, Mo, W)" @default.
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- W1977573766 doi "https://doi.org/10.1016/0020-1693(95)04513-9" @default.
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