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- W1977603922 abstract "GaPO 4 recrystallisation was studied under hydrothermal conditions at temperatures from 140 to 310°C (autogeneous pressures from 2 to 150 bar). The acidic solvents of pH 4 to 0 at ambient conditions were used as mineralizers. The retrograde solubility of GaPO 4 was observed under 260°C (pressure up to 20 bar) and direct - above 280°C (pressure above 50 bar). Low values of the initial solvent pH on GaPO 4 solubility at temperatures up to 260°C have an influence to increase GaPO 4 solubility and in the same time decrease crystalline quality, for example, rise of OH content is observed. Some solvents with pH near to 4 tested as mineralizers exhibit low solubility of GaPO 4 , but increasing value at temperatures above 280°C and lead to an attractive crystal growth. So, a possible explication of this phenomenon is a formation of few stable phases from an initial solution which can participate or no in reactions with GaPO 4 at certain T-P conditions. The study of crystalline quality and physical properties as well piezoelectric of GaPO 4 single crystals have shown a significant superiority of crystals obtained at temperatures above 280°C (pressures above 50 bar)." @default.
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- W1977603922 date "2005-06-01" @default.
- W1977603922 modified "2023-10-18" @default.
- W1977603922 title "The main features of GaPO4hydrothermal crystal growth under conditions of direct and retrograde solubility" @default.
- W1977603922 doi "https://doi.org/10.1051/jp4:2005126002" @default.
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