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- W1977759543 abstract "Performance of six quinolylazo compounds was studied as a pre-column derivatizing reagent for the separation of metal ions in the reversed-phase high-performance liquid chromatography. 2-(4-Methyl-2-quinolylazo)-5-diethylaminophenol (QADP) was suited for the determination of Co, Ni and Cu in the presence of a large amount of Fe. The detection limits under the optimized conditions [stationary phase: L-column ODS; mobile phase: acetone-water (62:38, v/v) containing 0.01 M NH4SCN and 0.01 M 2-morpholinoethanesulfonic acid-NaOH (pH 6); injection volume: 10 μl] were 0.24 ng for Co, 0.22 for Ni and 0.53 for Cu. This method was successfully applied to the determination of these metal ions in a standard steel sample." @default.
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- W1977759543 date "1997-12-01" @default.
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- W1977759543 title "Separation and simultaneous determination of cobalt, nickel and copper with 2-(4-methyl-2-quinolylazo)-5-diethylaminophenol by reversed-phase high-performance liquid chromatography" @default.
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- W1977759543 doi "https://doi.org/10.1016/s0039-9140(97)00135-5" @default.
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