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• W1977794592 endingPage "2437" @default.
• W1977794592 startingPage "2427" @default.
• W1977794592 abstract "An approach to the stereocontrolled synthesis of the protected form of sphingofungin E (32) starting from the known protected d-glucose derivative 3 is described herein. For the construction of a tetrasubstituted carbon atom that is substituted with nitrogen, the [3,3]-sigmatropic rearrangement of thiocyanate 8 was employed. Subsequent functional group interconversions afforded the highly functionalized fragment, allylic bromide 26. Its coupling reaction with the known C12 hydrophobic segment 2, followed by further manipulation, completed the total synthesis." @default.
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• W1977794592 date "2010-11-01" @default.
• W1977794592 modified "2023-09-27" @default.
• W1977794592 title "Total synthesis of a protected form of sphingofungin E using the [3,3]-sigmatropic rearrangement of an allylic thiocyanate as the key reaction" @default.
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• W1977794592 doi "https://doi.org/10.1016/j.carres.2010.09.016" @default.
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