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• W1977832682 abstract "Anatoxin-a (1) is the first neurotoxin obtained from a freshwater cyanobacterium, Anbaenaflos-aquae and has a high toxicity (LD50. i.p., mouse: 200 μg/kg). 1 has occurred limitedly in North America and northern Europe and no occurrence has bcen reported in Japan so far. Thermospray-liquid chromatography/mass spectrometry (TSP-LS/MS) was applied to the analysis of trace amount of 1 together with its degradation product (2) after the following optimizations: HPLC conditions, TSP operating conditions, slight modification of the reported clean-up method wings tandem cartridge system and introduction of acetyltropine as an internal standard. The established TSP-LC(MS is of great advantage to the conventional HPLC/UV and the detection limit was 500 pg. The method was used for trace analysis of 1 and 2 in laboratory strains and bloom samples and made possible the first detection of them in Japanese samples." @default.
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• W1977832682 date "1993-01-01" @default.
• W1977832682 modified "2023-10-18" @default.
• W1977832682 title "Liquid chromatography/mass spectrometric detection of anatoxin-a, a neurotoxin from cyanobacteria" @default.
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• W1977832682 doi "https://doi.org/10.1016/0040-4020(93)80011-h" @default.
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