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- W1978153208 abstract "Reductive coupling of 1-chloro-2-iodoperfluorocyclobutene (I), cyclopentene (III) and cyclohexene (VI) has been carried out with copper powder and a trace amount of dimethylformamide to give the corresponding 2,2′-dichloroperfluoro-(bi-1-cycloalken-1-yl) derivatives in 69%, 36% and 73% yield, respectively. A reduced by-product, 2H,2′H-dodecafluoro-(bi-1-cyclopenten-1-yl) was also obtained in the copper coupling of (III). Coupling of 1,2-di-iodoperfluorocyclobutene (IX) and cyclopentene (XII) under similar conditions gave good yields of cyclic trimers and tetramers. Mass spectra, infrared and 19F NMR data are discussed." @default.
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- W1978153208 date "1973-10-01" @default.
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- W1978153208 title "Copper coupling of 1-chloro-2-iodo- and 1,2-di-iodo-perfluorocycloalkenes" @default.
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- W1978153208 doi "https://doi.org/10.1016/s0022-1139(00)84159-7" @default.
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