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- W1978200967 abstract "Polychlorinated biphenyls (PCBs) were obtained by the partial catalytic dechlorination of individual PCBs having up to six chlorine atomes. The dechlorination was accomplished with sodium borohydride and nickel boride catalysis generated in situ. All of the expected PCB congeners were observed when decholorinating PCBs with four or less chlorine atoms. The mixtures were separated by gas chromatography on a methyl silicone capillary column. Identification of individual congeners was made by comparison of retention indices (RI) to literature, experimental and estimated values and by cross comparison of peaks generated from different parent PCBs. Various methods of estimating RIs were evaluated. The effects of varying concentration and reaction time was studied along with the relative reactivity of chlorines in different positions. The partially dechlorinated PCB mixtures are particularly useful as retention time standards for PCBs with less than four chlorine atoms." @default.
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- W1978200967 date "1985-01-01" @default.
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- W1978200967 title "Polychlorinated biphenyl retention time standards obtained by chemical dechlorination of polychlorinated biphenyl isomers" @default.
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- W1978200967 doi "https://doi.org/10.1016/s0021-9673(01)90682-x" @default.
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