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- W1978331424 abstract "Abstract We report optimized synthetic procedures to cis-TMCDA and cis-cyclohexane-1,2-diamine. Our new two-step approach is an efficient and low-cost method for synthesizing the ligand cis-TMCDA. In the preparation of cis-cyclohexane-1,2-diamine, the crystallization of the unexpected intermediate cis-cyclohexane-1,2-diammonium hydrogensulfate ethylsulfate made the subsequent reactions easier in their workup, as nickel(II) chloride impurities were eliminated." @default.
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- W1978331424 date "2011-10-01" @default.
- W1978331424 modified "2023-09-25" @default.
- W1978331424 title "Synthesis of cis-TMCDA: Optimization and characterization of a key intermediate" @default.
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- W1978331424 doi "https://doi.org/10.1016/j.ica.2011.06.008" @default.
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