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- W1978382079 abstract "The title salt was obtained by a reaction of [TTF]3 [BF4]2 (TTF = tetrathiafulvalene) with [NMe4]2 [V(mnt)3] [mnt = 1,2-dicyanoethylene-1,2- dithiolate(2−)] in a mixture of 1,2-dichloroethane and acetonitrile (3:2 ν/ν). A single crystal X-ray analysis of it revealed a TTF columnar structure consisting of both TTF0 and the TTF·+ radical cation and the distorted octahedral geometry of the [V(mnt)3]2− anion. The salt crystallizes in a monoclinic system, space group C2/c with unit cell constants a = 25.428(3), b = 12.434(2), c = 25.477(3) Å, β = 92.428(3)° and Z = 8. The structure was solved by the direct method and refined, on the basis of 3854 [|Fo| > 3σ(F)] observed data, to an R value of 0.078. The salt e`xhibits electrical conductivity of 1.7 x 10−4 S cm−1 at 25°C for a compacted pellet." @default.
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- W1978382079 date "1989-03-01" @default.
- W1978382079 modified "2023-09-26" @default.
- W1978382079 title "Crystal structure and properties of [TTF]2.5[V(mnt)3 ]·0.5CH2ClCH2Cl[TTF = tetrathiafulvalene and mnt = 1,2-dicyanoethylene-1,2-dithiolate(2−)]" @default.
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- W1978382079 doi "https://doi.org/10.1016/s0020-1693(00)80541-1" @default.
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