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- W1978384940 abstract "Treatment of [Et4N]2[WSe4] with the trinuclear trigonal-bipyramidal copper(I) complexes [Cu3(μ3-X)2(μ-L)3]X [X = I, L = bis(diphenylphosphanyl)methane (dppm) (1a); X = Cl, L = bis(diphenylphosphanyl)amine (dppa) (1b)] affords the tetranuclear cluster compounds [(μ3-WSe4)Cu3(μ-X)(μ-L)2] [X = I, L = dppm (2a); X = Cl, L = dppa (2b)], which exhibit an open butterfly configuration. Interaction of [Et4N]2[WSe4] with [Cu(MeCN)4][PF6] and L gives the pentanuclear cluster compounds [(μ4-WSe4)Cu4(μ-L)4][PF6]2 [L = dppm (3a), dppa (3b)] which contain an open co-planar WCu4 core. The solid-state structures of cluster compounds 2a, 2b, and 3a have been established by X-ray crystallography. The nonlinear optical properties of 2a and 3a have been examined by z-scan techniques with 7-ns pulses at 532 nm. The pentanuclear co-planar cluster 3a exhibits a large optical limiting effect (the limiting threshold is about 0.40 J cm–2). (© Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2007)" @default.
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- W1978384940 date "2007-05-01" @default.
- W1978384940 modified "2023-10-01" @default.
- W1978384940 title "Syntheses, Structures and Optical Nonlinearities of Heteroselenometallic W–Se–Cu Cluster Compounds Containing Bridging Phosphane Ligands" @default.
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- W1978384940 doi "https://doi.org/10.1002/ejic.200601114" @default.
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