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- W1978487989 abstract "The experimental aspects of the “Grob splitless” sampling technique are discussed in terms of the sampling time, purge activation time, solvent type, sample size, column temperature, injector temperature and column flow-rate. Guidelines are developed for using and simplifying splitless sampling. Optimized experimental parameters are given from the results of optimization by simplex. Precision data for retention times and peak areas are shown to be 0.05 and 1% respectively, for an automated splitless capillary system." @default.
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- W1978487989 date "1978-10-01" @default.
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- W1978487989 title "Splitless sampling for capillary-column gas chromatography" @default.
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- W1978487989 doi "https://doi.org/10.1016/s0021-9673(00)89959-8" @default.
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