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- W1978506563 abstract "We describe the structural refinement of zeolite beta using the local structure obtained with the pair distribution function (PDF) method. A high quality synchrotron and two neutron scattering datasets were obtained on two samples of siliceous zeolite beta. The two polytypes that make up zeolite beta have the same local structure; therefore refinement of the two structures was possible using the same experimental PDF. Optimized structures of polytypes A and B were used to refine the structures using the program PDFfit. Refinements using only the synchrotron or the neutron datasets gave results inconsistent with each other but a cyclic refinement with the two datasets gave a good fit to both PDFs. The results show that the PDF method is a viable technique to analyze the local structure of disordered zeolites. However, given the complexity of most zeolite frameworks, the use of both X-ray and neutron radiation and high-resolution patterns is essential to obtain reliable refinements." @default.
- W1978506563 created "2016-06-24" @default.
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- W1978506563 date "2005-01-01" @default.
- W1978506563 modified "2023-10-18" @default.
- W1978506563 title "A pair distribution function analysis of zeolite beta" @default.
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- W1978506563 doi "https://doi.org/10.1016/j.micromeso.2004.07.040" @default.
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