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• W1978573242 abstract "We studied unsupported VxOy nanoparticles prepared by a novel nonaqueous route in the selective oxidation of n-butane to maleic anhydride. The evolution of the electronic and geometric structure of the material was characterized by X-ray photoemission spectroscopy, electron energy-loss spectroscopy, transmission electron microscopy, and electron diffraction before and after the reaction at different temperatures. A change from a water-mediated CC bond cracking functionality of the catalyst forming acetic acid to an oxidizing functionality resulting in maleic anhydride was observed. It was found that the particles underwent a radical modification of the geometric and electronic structure that finally resulted in V2O5 crystals. Experimentally derived conclusions are related to some conceptual claims from the literature." @default.
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• W1978573242 date "2005-12-10" @default.
• W1978573242 modified "2023-09-23" @default.
• W1978573242 title "Synthesis and functional verification of the unsupported active phase of VxOy catalysts for partial oxidation of n-butane" @default.
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• W1978573242 doi "https://doi.org/10.1016/j.jcat.2005.10.005" @default.
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