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- W1978590753 abstract "A new class of polar polysilabutanes with mono- or tri-(oxyethylene)phenyl groups on the silicon atom have been synthesized by anionic polymerization of silacyclobutanes having ω-(t-butyldimethylsilyl-protected) mono- or tri-(oxyethylene)phenyl groups and subsequent deprotection of the silyl groups. The monomers were synthesized by treatment of 1,1-dichlorosilacyclobutane with ω-(t-butyldimethylsilyl-protected) mono- or tri-(oxyethylene)phenyl Grignard reagents. Anionic polymerization of silacyclobutane was performed with butyllithium initiator in THF. t-Butyldimethylsilyl-protecting groups at polymer pendant groups were hydrolyzed with tetrabutyl ammonium fluoride in water-containing THF. The obtained polysilabutanes were soluble in a polar organic solvent such as methanol, and their mass distributions were analysed by matrix-assisted laser-desorption-ionization mass spectrometry (MALDI TOF MS). © 1998 John Wiley & Sons, Inc. J Polym Sci A: Polym Chem 36: 225–231, 1998" @default.
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- W1978590753 date "1998-01-30" @default.
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- W1978590753 title "Synthesis and characterization of polysilabutane having oligo(oxyethylene)phenyl groups on the silicon atom" @default.
- W1978590753 doi "https://doi.org/10.1002/(sici)1099-0518(19980130)36:2<225::aid-pola3>3.0.co;2-q" @default.
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