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• W1978644460 abstract "The molecular structure of [1.1.1]propellane has been determined from single-crystal X-ray diffraction measurements at 138 K. The crystals of this reactive compound were grown from the melt at ca. 263 K. The space group is C2, and the asymmetric unit contains four molecules. All have large thermal motion and two show orientational disorder as well. Because of these problems, the atomic positions cannot be determined with high accuracy. Within the experimental limits, the two ordered molecules have D3h symmetry, with corrected lengths of central and side bonds of ca. 1.60 Å and 1.53 Å, respectively. At lower temperature, the crystals undergo a phase transition. The transition temperature, in the range of 100 to 132 K, varied from one crystal sample to another. All crystals obtained of the low-temperature phase were twinned, and its space group could not be established." @default.
• W1978644460 created "2016-06-24" @default.
• W1978644460 creator A5023710002 @default.
• W1978644460 date "1990-09-19" @default.
• W1978644460 modified "2023-10-07" @default.
• W1978644460 title "The crystal structure of [1.1.1]propellane at 138 K" @default.
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• W1978644460 doi "https://doi.org/10.1002/hlca.19900730603" @default.
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