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- W1978741540 abstract "(1→6)-α-Linked heteropolysaccharides composed of D-glucose and 2,3,4-trideoxy-DL-glycero-hexopyranose units were synthesized by cationic ring-opening copolymerization of 1,6-anhydro-2,3,4-tri-O-beazyl-β-D-glucose (TBLG) with rac-4(e)-bromo-6,8-dioxabicyclo[3.2.1]octane (BrDBO) followed by reductive debromination and subsequent debenzylation. The heteropolysaccharides (mole fraction of D-glucose unit, 0.34–0.90) were soluble in water and dimethyl sulfoxide, and insoluble in other organic solvents. Hydrolysis of the hetero-polysaccharides by an endodextranase from a Penicillium species was examined in an acetate buffer solution (pH 5.3) at 37°C. The maximum degree of hydrolysis based on the D-glucose units, (D.H.)D, decreased significantly with increasing 2,3,4-trideoxy-DL-glycero-hexopyranose units. The observed (D.H.)D values were in agreement with those calculated from the diad fractions of the original TBLG-BrDBO copolymers by a statistical treatment previously proposed for the enzymatic hydrolysis of DL-dextran." @default.
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- W1978741540 date "1987-05-01" @default.
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- W1978741540 title "Chemical Synthesis of Polysaccharides. VIII. Synthesis and Enzymatic Hydrolysis of (1→6)-α-Linked Heteropolysaccharides Consisting of D-Glucose and 2,3,4-Trideoxy-DL-glycero-hexopyranose Units" @default.
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- W1978741540 doi "https://doi.org/10.1295/polymj.19.581" @default.
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