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- W1978889130 abstract "Endfunctionalized polyisoprenes (PI) and polystyrenes (PS) with either one sulfonate or ammonium end group and α,ω-macrozwitterionic PI and PS have been synthesized and investigated by CW-EPR using the spin probe technique. From the extrema separation of the temperature dependent spectra a characteristic temperature, T‘50G, is introduced which can be employed as a measure for the temperature dependence of the chain end association in these telechelic ionomers. In this way it is shown that the mobility of an ionic 2,2,6,6-tetramethylpiperidine-N-oxyl derivative is dramatically restricted when compared to the corresponding nonionic probe. For PI the reduction in probe mobility corresponds to temperature shifts as high as 140 K relative to the dynamics of the polymer, indicating the presence of highly immobilized ion multiplets. As shown by the temperature dependent data, the method is sensitive to additional immobilization of the ionic domains induced by bulky substituents adjacent to the ionic chain ends. ..." @default.
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- W1978889130 date "1997-06-01" @default.
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- W1978889130 title "EPR Studies on Telechelic Polymers: Characterization of Ion Multiplets" @default.
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- W1978889130 doi "https://doi.org/10.1021/ma961591+" @default.
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