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• W1979040124 endingPage "2957" @default.
• W1979040124 startingPage "2953" @default.
• W1979040124 abstract "Treatment of acetonitrile solutions of [{Fe(CO)2(cp)}2EX2](cp =η-C5H5; E = Ge, X = Br; E = Sn, X = Cl) with an excess of sodium azide affords the compounds [{Fe(CO)2(cp)}2E(N3)2](E = Ge or Sn). X-Ray crystallographic analyses of these compounds show that the Group 14 atom has a distorted-tetrahedral environment, with enlarged Fe–E–Fe angles and reduced N–E–N angles. Contributions from various resonance forms of the azide ligand are discussed, based on the solid-state data, and are compared to expectations based on solid-state and solution νasym.(N3) and ν(CO) i.r. stretching frequencies." @default.
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• W1979040124 date "1990-01-01" @default.
• W1979040124 modified "2023-10-16" @default.
• W1979040124 title "Synthesis and characterization of transition-metal-substituted germanium and tin azides: X-ray crystal structures of [{Fe(CO)₂(cp)}₂E(N₃)₂](cp =η-C₅H₅, E = Ge or Sn)" @default.
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• W1979040124 doi "https://doi.org/10.1039/dt9900002953" @default.
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