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- W1979272014 abstract "Two new acyclic, potentially binucleating amide-containing ligands.H3L1 andH3L2, have been synthesised from the reaction of 4-methylphenol-2,6-diacyl chloride with an excess of 1,2-diaminobenzene or of 1,2-diamino-4,5-dimethylbenzene, respectively. Dicopper(II) complexes, [Cu2(L1)(X)] where X = CH3COO− or OH−, ahve been made fromH3L1 but the analogous nickel complexes could not be prepared and no complexes with either copper or nickel could be prepared fromH3L2. Interestingly, Schiff-base macrocyclic complexes derived from reactions ofH3L1 andH3L2 with 2,6-diformyl-4-methylphenol, 4-t-butyl-2,6-diformylphenol, or S-(2,6-diformyl-4-methyl-phenyl)-dimethylthiocarbamate, were successfully templated using these same two metal ions and resulted in the isolation of nine dimetallic complexes. A variety of structural modifications were made to the macrocycles via the choice dialdehyde precursor, including changing a phenolate bridge for a thiophenolate one, in an attempt to increase the solubility of the products." @default.
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- W1979272014 date "1998-11-01" @default.
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- W1979272014 title "Binuclear nickel(II) and copper(II) complexes of amide-containing two-armed and macrocyclic ligands" @default.
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- W1979272014 doi "https://doi.org/10.1016/s0020-1693(98)00240-0" @default.
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