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• W1979280210 abstract "We show that the structure factor S(q) of water can be obtained from x-ray synchrotron experiments at grazing angle of incidence (in reflection mode) by using a liquid surface diffractometer. The corrections used to obtain S(q) self-consistently are described. Applying these corrections to scans at different incident beam angles (above the critical angle) collapses the measured intensities into a single master curve, without fitting parameters, which within a scale factor yields S(q). Performing the measurements below the critical angle for total reflectivity yields the structure factor of the top most layers of the water/vapor interface. Our results indicate water restructuring at the vapor/water interface. We also introduce a new approach to extract g(r), the pair distribution function (PDF), by expressing the PDF as a linear sum of error functions whose parameters are refined by applying a nonlinear least square fit method. This approach enables a straightforward determination of the inherent uncertainties in the PDF. Implications of our results to previously measured and theoretical predictions of the PDF are also discussed." @default.
• W1979280210 created "2016-06-24" @default.
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• W1979280210 date "2008-07-24" @default.
• W1979280210 modified "2023-10-16" @default.
• W1979280210 title "Extracting the pair distribution function of liquids and liquid-vapor surfaces by grazing incidence x-ray diffraction mode" @default.
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• W1979280210 doi "https://doi.org/10.1063/1.2953572" @default.
• W1979280210 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/18681657" @default.
• W1979280210 hasPublicationYear "2008" @default.
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