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• W1979280319 endingPage "642" @default.
• W1979280319 startingPage "637" @default.
• W1979280319 abstract "The i.r. and Raman spectra including Raman single crystal measurements of the isostructural Ba(ClO3)2·H2O, Ba(BrO3)2·H2O, Sr(BrO3)2·H2O, and Sr(IO3)2·H2O and of Ba(ClO3)2·H2O-Ba(BrO3)2·H2O solid solutions are presented in the water band and the XO stretching mode region at 90 and 295 K. Assignment of the XO stretching modes to the intramolecular vibrations v1 and v3 of the halate ions and the species of the unit cell group C2h is performed and discussed in terms of the relative intensity of the i.r. and Raman bands, the frequency shifting among the halate monohydrates, the single crystal Raman spectra and the spectra of matrix isolated ClO−3 and BrO−3 ions. The effective XO stretching force constants are in the order ClO−3 > lO−3 > BrO−3. The order of v1 and v3 is v1 < v3 for ClO−3 and v1 > v3 for BrO−3 and IO−3·.33Cl/37Cl isotopic splitting of the ClO stretching modes, as discussed formerly, can be excluded. The spectra of matrix isolated ClO3−3 and BrO−3 ions (site symmetry C1) show three XO stretching bands (one v1 and two v3). The frequency shifting of the OH stretching modes resembles that of other isostructural solid hydrates with weak hydrogen bonds. It can be correlated to the repulsion potential of the lattice and the metal—water interaction." @default.
• W1979280319 created "2016-06-24" @default.
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• W1979280319 date "1985-01-01" @default.
• W1979280319 modified "2023-10-16" @default.
• W1979280319 title "Infrared and single crystal Raman studies of alkaline earth chlorate, bromate and iodate monohydrates and of halate ions matrix isolated in Ba(ClO3)2·H2Otype host lattices" @default.
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• W1979280319 doi "https://doi.org/10.1016/0584-8539(85)80051-9" @default.
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