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- W1979319573 abstract "Multilayer capacitors with thin, dielectric BaTiO3 layers can possess a relatively high capacitance per unit volume. A solid metallic precursor method has recently been developed for preparing thin BaTiO3/noble metal laminates. In the present paper, the phase and microstructural evolution of Ba-Ti metallic precursors were examined after oxidation at 300° to 900°C in pure oxygen at 1 atm pressure. Barium peroxide, BaO2, formed rapidly during oxidation at 300°C, with titanium largely remaining as unoxidized particles in the peroxide matrix. Between 375° and 500°C, the solidstate reaction of barium peroxide with metallic titanium yielded barium orthotitanate, Ba2TiO4. Further exposure to temperatures between 500° and 900°C resulted in the oxidation of residual metallic titanium. The oxidized titanium then reacted with the orthotitanate matrix to form barium metatitanate, BaTiO3. The rate of formation of BaTiO3 was found to be strongly dependent on the degree of milling of the Ba-Ti precursors and on the heating rate between 300° and 500°C." @default.
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- W1979319573 date "1994-03-01" @default.
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- W1979319573 title "A Novel Reaction Path to BaTiO3 by the Oxidation of a Solid Metallic Precursor" @default.
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- W1979319573 doi "https://doi.org/10.1111/j.1151-2916.1994.tb05356.x" @default.
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