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- W1979542440 abstract "The Bamberger-Ham condensation of 4-substituted nitrosobenzenes in concentrated sulfuric acid reported as a method of synthesis for phenazine N-oxides has been found to be limited to electron donating substituents. Methyl 4-nitrosobenzoale has been found to react under these conditions to give dimethyl 2-nitrodiphenylamine-4, 5-diearboxylate (2). Compounds of unknown structure previously reported to arise from acid treatment of 4-bromo- and 4-chloronilrosobenzene have been shown to be 4, 5-dibromo-2-nitrosophenylamine (10) and the analogous dichloro compound. Treatment under stronger acidic conditions (oleum) converted 10 but not 2 into the corresponding phenazine N-oxide. Mechanistic implications are discussed." @default.
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- W1979542440 date "1979-03-01" @default.
- W1979542440 modified "2023-09-25" @default.
- W1979542440 title "A reinvestigation of the bamberger-ham phenazine. Synthesis: A limitation" @default.
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- W1979542440 doi "https://doi.org/10.1002/jhet.5570160243" @default.
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